Grain growth modeling for gas pressure sintering of silicon nitride based ceramics
Résumé
The complexity of liquid phase sintering of silicon nitride implies the use of advanced gas
pressure sintering (GPS) industrial process. Sintering additives have been jointly developed to
allow the sintering of this challenging material to reach high mechanical properties. The latter
properties and GPS process of silicon nitride are strongly influenced by the microstructure
development during the thermal treatment under temperature close to 1800°C. In particular,
grain growth is a key parameter that needs to be identified. In this work, an experimental
design is used to explore microstructural development during the final stage of sintering. The
grain size, and porosity data are extracted for different holding times and temperatures to
allow the identification of the experimental grain growth. The study is extended to the impact
of the heating kinetics regime and the influence of the gas pressure furnace environment.
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