Resistive-nanoindentation on gold: Experiments and modeling of the electrical contact resistance
Résumé
This paper reports the experimental, analytical, and numerical study of resistive-nanoindentation tests performed on gold samples (bulk and
thin film). First, the relevant contributions to electrical contact resistance are discussed and analytically described. A brief comparison of tests
performed on gold and on natively oxidized metals highlights the high reproducibility and the voltage-independence of experiments on gold
(thanks to its oxide-free surface). Then, the evolution of contact resistance during nanoindentation is fully explained in terms of electronic
transport regimes: starting from tunneling, electronic transport is then driven by ballistic conduction before ending with pure diffusive con-
duction. The corresponding analytical expressions, as well as their validity domains, are determined and compared with experimental data,
showing excellent agreement. From there, focus is made on the diffusive regime. Resistive-nanoindentation outputs are fully described by
analytical and finite-element modeling. The developed numerical framework allows a better understanding of the main parameters: it first
assesses the technique capabilities (validity domains, sensitivity to tip defect, sensitivity to rheology, effect of an oxide layer, and so on), but
it also validates the different assumptions made on current line distribution. Finally, it is shown that a simple calibration procedure allows a
well-resolved monitoring of the contact area during resistive-nanoindentation performed on samples with complex rheologies (ductile thin
film on an elastic substrate). Comparison to analytical and numerical approaches highlights the strength of resistive-nanoindentation for
continuous area monitoring.
Fichier principal
Resistive nanoindentation - Gold_RSI_Revised_HAL version.pdf (2.35 Mo)
Télécharger le fichier
Origine | Fichiers produits par l'(les) auteur(s) |
---|