Improving the reliability of small- and wide-angle X-ray scattering measurements of anisotropic precipitates in metallic alloys using sample rotation - Archive ouverte HAL
Article Dans Une Revue Journal of Applied Crystallography Année : 2024

Improving the reliability of small- and wide-angle X-ray scattering measurements of anisotropic precipitates in metallic alloys using sample rotation

Résumé

Nanometric precipitates in metallic alloys often have highly anisotropic shapes. Given the large grain size and non-random texture typical of these alloys, performing small-and wide-angle X-ray scattering (SAXS/WAXS) measurements on such samples for determining their characteristics (typically size and volume fraction) results in highly anisotropic and irreproducible data. Rotations of flat samples during SAXS/WAXS acquisitions are presented here as a solution to these anisotropy issues. Two aluminium alloys containing anisotropic precipitates are used as examples to validate the approach with a À 45 � /45 � angular range. Clear improvements can be seen on the SAXS I(q) fitting and the consistency between the different SAXS/WAXS measurements. This methodology results in more reliable measurements of the precipitate's characteristics, and thus allows for time-and space-resolved measurements with higher accuracy
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Dates et versions

hal-04781141 , version 1 (13-11-2024)

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Thomas Perrin, Gilbert A Chahine, Stéphan Arnaud, Arthur Després, Pierre Heugue, et al.. Improving the reliability of small- and wide-angle X-ray scattering measurements of anisotropic precipitates in metallic alloys using sample rotation. Journal of Applied Crystallography, 2024, 57 (Part 6), pp.1800-1814. ⟨10.1107/s1600576724009294⟩. ⟨hal-04781141⟩
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