Pair transfer is a unique tool to study pairing correlations in nuclei. Neutron-proton pairing is investigated in the N=Z nuclei of the f-shell, through the reaction (p,3He) in inverse kinematics, that allows to populate at the same time the lowest J=0+, T=1 (isovector pairing) state and J=1+, T=0 (isoscalar pairing) state. Radioactive beams of 56Ni and 52Fe produced by fragmentation at the GANIL/LISE facility combined with particle and gamma-ray detection make it possible to carry out this study from 48Cr (mid-shell nucleus) to 56Ni (doubly-magic nucleus). The cross-sections were extracted and compared with second-order distorted-wave born approximation (DWBA) calculations performed with neutron-proton amplitudes obtained from shell model calculations with GXPF1 interaction. Very low cross-sections for the J=1+,T=0 state (isoscalar channel) were observed. The cross-section for 56Ni is one of order of magnitude lower than for 40Ca showing a strong reduction of the isoscalar channel in the f-shell as compared to the sd-shell. On the other hand, the increase of the cross-section towards the middle of the shell for the isovector channel points towards a possible superfluid phase.