In-situ Laue micro-diffraction during compression tests on Ce-TZP single crystal micropillars
Résumé
The widespread use of ceramics faces challenges due to their limited ductility, stemming from a lack of dislocation-induced plasticity. This study focuses on ceria-stabilized tetragonal zirconia a ceramic that benefits from its unique tetragonal-to-monoclinic phase transformation under stress, leading to transformation-induced plasticity (TRIP). Employing a micro-scale in-situ approach, the study aims to understand the mechanisms governing TRIP, particularly focusing on crystallographic features of the transformation. In-situ compression tests using synchrotron light source and Laue micro-diffraction were conducted on single crystal micropillars with various orientations. Results show that crystal orientation significantly affects the mechanical behaviour, with transformation being most likely when the resolved shear stress on {100} planes of the double-cell and along the <010> direction is highest. The martensite theory validates the correspondences obtained experimentally. This research provides insights into enhancing the mechanical properties of ceramics by leveraging the TRIP mechanisms.