From Amorphous Red Phosphorus to a Few Layers of Black Phosphorus: A Low-cost and Efficient Preparation Process - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Jordan Journal of Physics Année : 2019

From Amorphous Red Phosphorus to a Few Layers of Black Phosphorus: A Low-cost and Efficient Preparation Process

G Tiouitchi
  • Fonction : Auteur
F Elmanjli
  • Fonction : Auteur
O Mounkachi
  • Fonction : Auteur
A Mahmoud
  • Fonction : Auteur
F Boschini
  • Fonction : Auteur
A Kara
  • Fonction : Auteur
H Oughaddou
M Hamedoun
  • Fonction : Auteur
A Benyoussef
  • Fonction : Auteur
M Ait Ali
  • Fonction : Auteur

Résumé

In this work, we present an efficiency synthesis method of phosphorene from red phosphorus by means of black phosphorus. The latter was synthesized by using copper, tin, tin iodide and red phosphorus as precursor at low pressure-temperature. Characterizations with powder X-ray diffraction, scanning electron microscopy (SEM), energy dispersive spectrometry (EDX), high-resolution TEM (HR-TEM) and Raman spectroscopy were performed to confirm the high quality and purity of black phosphorus crystal. Liquid phase method was used to exfoliate black phosphorus to phosphorene in N-methyl-2-pyrrolidone (NMP) as solvent. Atomic force microscopy and STEM were used to confirm the exfoliation of black phophorus in a few layers of phophorene.

Domaines

Chimie
Fichier principal
Vignette du fichier
Jordan_Journal_physics_Phosphorene.pdf (1.43 Mo) Télécharger le fichier
Origine : Fichiers éditeurs autorisés sur une archive ouverte

Dates et versions

hal-04382306 , version 1 (09-01-2024)

Identifiants

Citer

G Tiouitchi, F Elmanjli, O Mounkachi, A Mahmoud, F Boschini, et al.. From Amorphous Red Phosphorus to a Few Layers of Black Phosphorus: A Low-cost and Efficient Preparation Process. Jordan Journal of Physics, 2019, ⟨10.47011/13.2.6 Authors:⟩. ⟨hal-04382306⟩
7 Consultations
20 Téléchargements

Altmetric

Partager

Gmail Facebook X LinkedIn More