Poly(ethylene glycol)s as grinding additives in the mechanochemical preparation of highly functionalized 3,5-disubstituted hydantoins - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Beilstein Journal of Organic Chemistry Année : 2017

Poly(ethylene glycol)s as grinding additives in the mechanochemical preparation of highly functionalized 3,5-disubstituted hydantoins

Andrea Mascitti
  • Fonction : Auteur
Massimiliano Lupacchini
  • Fonction : Auteur
Ruben Guerra
  • Fonction : Auteur
Ilya Taydakov
Lucia Tonucci
  • Fonction : Auteur
Nicola D’alessandro
  • Fonction : Auteur
Jean Martinez
  • Fonction : Auteur
Evelina Colacino
  • Fonction : Auteur
  • PersonId : 1086275

Résumé

The mechanochemical preparation of highly functionalized 3,5-disubstituted hydantoins was investigated in the presence of various poly(ethylene) glycols (PEGs), as safe grinding assisting agents (liquid-assisted grinding, LAG). A comparative study under drygrinding conditions was also performed. The results showed that the cyclization reaction was influenced by the amount of the PEG grinding agents. In general, cleaner reaction profiles were observed in the presence of PEGs, compared to dry-grinding procedures.
Fichier principal
Vignette du fichier
113-2017-BJOC.pdf (335.74 Ko) Télécharger le fichier
Origine Fichiers éditeurs autorisés sur une archive ouverte

Dates et versions

hal-03079220 , version 1 (17-12-2020)

Identifiants

Citer

Andrea Mascitti, Massimiliano Lupacchini, Ruben Guerra, Ilya Taydakov, Lucia Tonucci, et al.. Poly(ethylene glycol)s as grinding additives in the mechanochemical preparation of highly functionalized 3,5-disubstituted hydantoins. Beilstein Journal of Organic Chemistry, 2017, 13, pp.19 - 25. ⟨10.3762/bjoc.13.3⟩. ⟨hal-03079220⟩
29 Consultations
37 Téléchargements

Altmetric

Partager

Gmail Mastodon Facebook X LinkedIn More