Efficient synthesis of chiral γ-aminobutyric esters via direct rhodium-catalysed enantioselective hydroaminomethylation of acrylates - Archive ouverte HAL
Article Dans Une Revue Catalysis Science & Technology Année : 2020

Efficient synthesis of chiral γ-aminobutyric esters via direct rhodium-catalysed enantioselective hydroaminomethylation of acrylates

Résumé

The successful rhodium catalysed asymmetric intermolecular hydroaminomethylation (HAM) of alkenes using a single catalyst bearing the (R,R)-QuinoxP* ligand is reported. The HAM of α-alkyl acrylates is revealed to be an efficient tool for the regio- and enantioselective synthesis of γ-amino esters with ees up to 86%. HPNMR experiments provided insights into the reaction mechanism.
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Dates et versions

hal-02877761 , version 1 (22-06-2020)

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Citer

Anton Cunillera, Miriam Díaz de Los Bernardos, Martine Urrutigoity, Carmen Claver, Aurora Ruiz, et al.. Efficient synthesis of chiral γ-aminobutyric esters via direct rhodium-catalysed enantioselective hydroaminomethylation of acrylates. Catalysis Science & Technology, 2020, 10 (3), pp.630-634. ⟨10.1039/C9CY01797F⟩. ⟨hal-02877761⟩
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