High-resolution (1)H homonuclear dipolar recoupling NMR spectra of biological solids at MAS rates up to 67 kHz - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Journal of Magnetic Resonance Année : 2009

High-resolution (1)H homonuclear dipolar recoupling NMR spectra of biological solids at MAS rates up to 67 kHz

Denis Schneider
  • Fonction : Auteur
Fabien Aussenac

Résumé

Two-dimensional 1H homonuclear correlation NMR spectra of solids of biological interest have been recorded at high magnetic fields (14.1 and 18.8 T) and MAS rates up to 67 kHz, using symmetry-based homonuclear recoupling and CRAMPS decoupling; this method affords exceptional spectral resolution and is well suited to probe 1H–1H proximities in powdered solids.

Dates et versions

hal-01711610 , version 1 (18-02-2018)

Identifiants

Citer

Luis Mafra, Renée Siegel, Christian Fernandez, Denis Schneider, Fabien Aussenac, et al.. High-resolution (1)H homonuclear dipolar recoupling NMR spectra of biological solids at MAS rates up to 67 kHz. Journal of Magnetic Resonance, 2009, 199 (1), pp.111-114. ⟨10.1016/j.jmr.2009.04.004⟩. ⟨hal-01711610⟩
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