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Journal Articles Accreditation and Quality Assurance Year : 2009

Development of a reference measurement procedure for the determination of methylmercury in fish products

Abstract

The development of an analytical procedure for speciation analysis of methylmercury in fish products is presented. The method is based on high-performance liquid chromatography hyphenated to inductively coupled plasma-mass spectrometry. The metrological approach is stressed out in this paper, in order to provide reliable and comparable results. A complete uncertainty budget has been evaluated and the method has been validated by the use of a certified reference material. Moreover, the detection could rely on the isotope dilution mass spectrometry, a powerful strategy capable of highly accurate results traceable to the "Système International d'Unités" and recognised by the "Comité Consultatif pour la Quantité de Matière" as a primary method of measurement. © 2009 Springer-Verlag.
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hal-01561276 , version 1 (12-07-2017)

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S. Sannac, P. Fisicaro, G. Labarraque, Florence Pannier, M. Potin-Gautier. Development of a reference measurement procedure for the determination of methylmercury in fish products. Accreditation and Quality Assurance, 2009, 14 (5), pp.263-267. ⟨10.1007/s00769-009-0509-8⟩. ⟨hal-01561276⟩

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