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Article Dans Une Revue Talanta Année : 2012

Capillary electrophoresis with electrospray ionisation-mass spectrometry for the characterisation of degradation products in aged papers

Résumé

A methodology for capillary electrophoresis/electrospray ionisation mass spectrometry (CE/ESI-MS) was developed for the simultaneous analysis of degradation products from paper among two families of compounds: low molar mass aliphatic organic acids, and aromatic (phenolic and furanic) compounds. The work comprises the optimisation of the CE separation and the ESI-MS parameters for improved sensitivity with model compounds using two successive designs of experiments. The method was applied to the analysis of lignocellulosic paper at different stages of accelerated hygrothermal ageing. The compounds of interest were identified. Most of them could be quantified and several additional analytes were separated.
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Dates et versions

hal-01491170 , version 1 (22-03-2017)

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Anne-Laurence Dupont, Agathe Seemann, Bertrand Lavédrine. Capillary electrophoresis with electrospray ionisation-mass spectrometry for the characterisation of degradation products in aged papers. Talanta, 2012, 89, pp.301-309. ⟨10.1016/j.talanta.2011.12.032⟩. ⟨hal-01491170⟩

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