Article Dans Une Revue Journal of Saudi Chemical Society Année : 2012

Synthesis, characterization and coordination chemistry of substituted β-amino dicarbonyls

Résumé

An efficient and facile method for the synthesis of novel structurally diverse β-amino dicarbonyl compounds is described by exploring the aza-Michael addition reaction in an aqueous medium as a key step. Thereby, 2-(aryl-disubstituted-amino-1-yl-methyl)-malonic acid diethyl esters were achieved in a good to excellent yields. These products were easily isolated with enough purity just by using simple recrystallization. The crystals of the compounds (17) and (24) have been obtained and studied by X-ray crystallographic analyses.

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hal-00855345 , version 1 (29-08-2013)

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Ihssan Meskini, Maria Daoudi, Abdelali Kerbal, Brahim Bennani, Javed Sheikh, et al.. Synthesis, characterization and coordination chemistry of substituted β-amino dicarbonyls. Journal of Saudi Chemical Society, 2012, 16 (2), pp.161-173. ⟨10.1016/j.jscs.2010.12.005⟩. ⟨hal-00855345⟩
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