Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material - Archive ouverte HAL
Article Dans Une Revue Chemical Science Année : 2023

Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material

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Solid-state DNP NMR is applied to detect a small amount of a minor polymorph of an organic material within a major polymorphic phase, yielding quantitative details of the spatial distribution of the two polymorphs within particles in a powder sample.
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hal-04302638 , version 1 (23-11-2023)

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Samuel F Cousin, Colan E Hughes, Fabio Ziarelli, Stéphane Viel, Giulia Mollica, et al.. Exploiting solid-state dynamic nuclear polarization NMR spectroscopy to establish the spatial distribution of polymorphic phases in a solid material. Chemical Science, 2023, 14 (37), pp.10121-10128. ⟨10.1039/D3SC02063K⟩. ⟨hal-04302638⟩
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