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Article Dans Une Revue Mediterranean Journal of Chemistry Année : 2023

Crystal structure of cyclohexylammonium hydrogen maleate salt hemi-hydrated

Résumé

The compound CyNH3[HOOC(CH)2COO]•H2O has been obtained using one pot-synthesis process by mixing, in methanol, HOOC(CH)2COOH, CyNH2 and SnPh3Cl in a 1:1:1 molar ratio. X-ray diffraction analysis of the compound reveals that in the crystal structure, hydrogen maleate [HOOC(CH)2COO]-in cis configuration interacts with [CyNH3] + cations and water molecules to generate an R6 6 (22) ring. The interconnections of the rings via simple (N-H••O and O-H••O) and bifurcated (N-H•••(O, O)) hydrogen bonds give rise to a 2D supramolecular structure.
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Dates et versions

hal-03946684 , version 1 (19-01-2023)

Identifiants

Citer

Boucar Diouf, Bougar Sarr, Waly Diallo, Mouhamadou Sembéne Boye, Cheikh Abdoul Khadir Diop, et al.. Crystal structure of cyclohexylammonium hydrogen maleate salt hemi-hydrated. Mediterranean Journal of Chemistry, 2023, 13 (1), pp.1-7. ⟨10.13171/mjc02301041662diallo⟩. ⟨hal-03946684⟩
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