Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12)
Résumé
Automated X-ray data recording and data reduction strategies are straightforward and powerful these days, as well as semi-automated routines to solve standard structures without, or at least with only little manual intervention and within a relatively short time. The structure determination of the amino-carborane closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12), C 22 H 29 B 10 N, is an example that automated routines still always have to be revised and that it may be necessary to be aware of possible problems of a structure determination.
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Milewski, Pitfalls of a structure determination, 2022.pdf (964.33 Ko)
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10.1107S205698902201043X Original Data.zip (47.55 Mo)
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