Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12) - Archive ouverte HAL Access content directly
Journal Articles Acta crystallographica Section E : Crystallographic communications [2015-...] Year : 2022

Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12)

Abstract

Automated X-ray data recording and data reduction strategies are straightforward and powerful these days, as well as semi-automated routines to solve standard structures without, or at least with only little manual intervention and within a relatively short time. The structure determination of the amino-carborane closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12), C 22 H 29 B 10 N, is an example that automated routines still always have to be revised and that it may be necessary to be aware of possible problems of a structure determination.
Fichier principal
Vignette du fichier
Milewski, Pitfalls of a structure determination, 2022.pdf (964.33 Ko) Télécharger le fichier
10.1107S205698902201043X Original Data.zip (47.55 Mo) Télécharger le fichier
Origin Publication funded by an institution

Dates and versions

hal-03875823 , version 1 (28-11-2022)

Licence

Identifiers

Cite

Max Milewski, Anne-Marie Caminade, Evamarie Hey-Hawkins, Peter Lönnecke. Pitfalls of a structure determination: The structure of closo -9-[4-(dibenzylamino)phenyl]-1,2-dicarbadodecaborane(12). Acta crystallographica Section E : Crystallographic communications [2015-..], 2022, 78 (12), pp.1145-1150. ⟨10.1107/S205698902201043X⟩. ⟨hal-03875823⟩
88 View
52 Download

Altmetric

Share

Gmail Mastodon Facebook X LinkedIn More