Improved high-resolution EBSD analyses by correcting radial distortion of electron diffraction patterns - Archive ouverte HAL
Article Dans Une Revue Materials Characterization Année : 2022

Improved high-resolution EBSD analyses by correcting radial distortion of electron diffraction patterns

Résumé

Registering experimental and simulated electron diffraction patterns is increasingly used for advanced electron backscatter diffraction indexation (EBSD) analysis, yet the accuracy of registration is limited by several effects not accounted for in pattern simulation, such as the Kikuchi band (K-band) asymmetry, gray level reversal and (mainly radial) optical distortion. Radial distortion parameters have previously been measured with chessboardtype standard samples. Simulated patterns have been adopted to demonstrate the necessity of optical distortion removal in EBSD analyses. However there still lacks an efficient and precise radial distortion assessment and correction method. Here a simple radial distortion model, including barrel and pincushion distortions, is proposed to rectify the diffraction patterns during EBSD analyses. The correlation between experimental pattern and the simulated master pattern permits to index the diffraction pattern and assess the radial distortion simultaneously. The method is applied to three high-definition experimental electron diffraction datasets acquired with different cameras. The radial distortion parameter is identified with a relative uncertainty below 4%. The consideration of radial distortion improves the correlation between experimental and simulated patterns. Gray level profiles of the K-bands are analyzed to verify the correctness of image registration. The current method provides a fast, economic yet precise correction of the radial distortion for advanced EBSD analyses.
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Dates et versions

hal-03860934 , version 1 (18-11-2022)

Identifiants

  • HAL Id : hal-03860934 , version 1

Citer

Qiwei Shi, Emeric Plancher, Dominique Loisnard, Phani Karamched, Liu Jun, et al.. Improved high-resolution EBSD analyses by correcting radial distortion of electron diffraction patterns. Materials Characterization, 2022, 194, pp.112458. ⟨hal-03860934⟩
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