2,3,5-Tri-O-benzyl-D-xylofuranose
Résumé
The synthesis and crystallization of 2,3,5-tri-O-benzyl-D-xylofuranose permitted us to isolate the alpha anomer with a small contamination of the beta form (ca 10%), whose first crystallographic structure obtained in the P2$_1$2$_1$2$_1$ space group was determined at 100 K up to a resolution of sin θmax/λ = 0.71 Å$^{−1}$ and refined to an R1 value of 0.0171 with a Hirshfeld atom refinement (HAR) approach
Origine | Fichiers éditeurs autorisés sur une archive ouverte |
---|