<?xml version="1.0" encoding="utf-8"?>
<TEI xmlns="http://www.tei-c.org/ns/1.0" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:hal="http://hal.archives-ouvertes.fr/" xmlns:gml="http://www.opengis.net/gml/3.3/" xmlns:gmlce="http://www.opengis.net/gml/3.3/ce" version="1.1" xsi:schemaLocation="http://www.tei-c.org/ns/1.0 http://api.archives-ouvertes.fr/documents/aofr-sword.xsd">
  <teiHeader>
    <fileDesc>
      <titleStmt>
        <title>HAL TEI export of hal-03642105</title>
      </titleStmt>
      <publicationStmt>
        <distributor>CCSD</distributor>
        <availability status="restricted">
          <licence target="https://creativecommons.org/publicdomain/zero/1.0/">CC0 1.0 - Universal</licence>
        </availability>
        <date when="2026-05-16T14:34:08+02:00"/>
      </publicationStmt>
      <sourceDesc>
        <p part="N">HAL API Platform</p>
      </sourceDesc>
    </fileDesc>
  </teiHeader>
  <text>
    <body>
      <listBibl>
        <biblFull>
          <titleStmt>
            <title xml:lang="en">Synthesis of 0.94 Na0.5Bi0.5TiO3 – 0.06 BaTiO3 (NBT-6BT) lead-free piezoelectric powder suitable for aerosol deposition (AD)</title>
            <author role="aut">
              <persName>
                <forename type="first">Innocent</forename>
                <surname>Nomel</surname>
              </persName>
              <idno type="idhal" notation="numeric">807285</idno>
              <idno type="halauthorid" notation="string">2213717-807285</idno>
              <idno type="ORCID">https://orcid.org/0000-0003-4418-5927</idno>
              <affiliation ref="#struct-1089379"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Jérôme</forename>
                <surname>Lelievre</surname>
              </persName>
              <idno type="halauthorid">2478060-0</idno>
              <affiliation ref="#struct-1089379"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Laurence</forename>
                <surname>Boyer</surname>
              </persName>
              <idno type="halauthorid">651434-0</idno>
              <affiliation ref="#struct-73554"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Olivier</forename>
                <surname>Durand-Panteix</surname>
              </persName>
              <idno type="idhal" notation="numeric">773064</idno>
              <idno type="halauthorid" notation="string">883641-773064</idno>
              <idno type="ORCID">https://orcid.org/0000-0003-3926-0064</idno>
              <affiliation ref="#struct-73554"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Pascal</forename>
                <surname>Marchet</surname>
              </persName>
              <email type="md5">5f835411b89ba245df256cf246a6589c</email>
              <email type="domain">unilim.fr</email>
              <idno type="idhal" notation="string">pascal-marchet</idno>
              <idno type="idhal" notation="numeric">1851</idno>
              <idno type="halauthorid" notation="string">15707-1851</idno>
              <idno type="ORCID">https://orcid.org/0000-0001-6694-6120</idno>
              <idno type="IDREF">https://www.idref.fr/127468765</idno>
              <idno type="VIAF">https://viaf.org/viaf/196193268</idno>
              <idno type="ISNI">http://isni.org/isni/0000000138772469</idno>
              <affiliation ref="#struct-522021"/>
            </author>
            <editor role="depositor">
              <persName>
                <forename>Pascal</forename>
                <surname>Marchet</surname>
              </persName>
              <email type="md5">5f835411b89ba245df256cf246a6589c</email>
              <email type="domain">unilim.fr</email>
            </editor>
          </titleStmt>
          <editionStmt>
            <edition n="v1" type="current">
              <date type="whenSubmitted">2022-04-14 18:10:12</date>
              <date type="whenModified">2025-07-02 07:22:02</date>
              <date type="whenReleased">2022-04-14 18:24:54</date>
              <date type="whenProduced">2022</date>
              <date type="whenEndEmbargoed">2022-04-14</date>
              <ref type="file" target="https://hal.science/hal-03642105v1/document">
                <date notBefore="2022-04-14"/>
              </ref>
              <ref type="file" subtype="author" n="1" target="https://hal.science/hal-03642105v1/file/Manuscrit%20-%20CERI-.pdf" id="file-3642105-3180987">
                <date notBefore="2022-04-14"/>
              </ref>
            </edition>
            <respStmt>
              <resp>contributor</resp>
              <name key="192905">
                <persName>
                  <forename>Pascal</forename>
                  <surname>Marchet</surname>
                </persName>
                <email type="md5">5f835411b89ba245df256cf246a6589c</email>
                <email type="domain">unilim.fr</email>
              </name>
            </respStmt>
          </editionStmt>
          <publicationStmt>
            <distributor>CCSD</distributor>
            <idno type="halId">hal-03642105</idno>
            <idno type="halUri">https://hal.science/hal-03642105</idno>
            <idno type="halBibtex">nomel:hal-03642105</idno>
            <idno type="halRefHtml">&lt;i&gt;Ceramics International&lt;/i&gt;, 2022, 48 (10), pp.14697-14707. &lt;a target="_blank" href="https://dx.doi.org/10.1016/j.ceramint.2022.02.005"&gt;&amp;#x27E8;10.1016/j.ceramint.2022.02.005&amp;#x27E9;&lt;/a&gt;</idno>
            <idno type="halRef">Ceramics International, 2022, 48 (10), pp.14697-14707. &amp;#x27E8;10.1016/j.ceramint.2022.02.005&amp;#x27E9;</idno>
            <availability status="restricted">
              <licence target="https://about.hal.science/hal-authorisation-v1/">HAL Authorization<ref corresp="#file-3642105-3180987"/></licence>
            </availability>
          </publicationStmt>
          <seriesStmt>
            <idno type="stamp" n="UNILIM">Université de Limoges</idno>
            <idno type="stamp" n="CNRS">CNRS - Centre national de la recherche scientifique</idno>
            <idno type="stamp" n="SPCTS" corresp="UNILIM">Science des Procédés Céramiques et de Traitements de Surface</idno>
            <idno type="stamp" n="SPCTS-AXE3" corresp="SPCTS">Axe 3 : organisation structurale multiéchelle des matériaux</idno>
            <idno type="stamp" n="IPAM" corresp="UNILIM">Institut des Procédés Appliqués aux Matériaux</idno>
            <idno type="stamp" n="INC-CNRS">Institut de Chimie du CNRS</idno>
            <idno type="stamp" n="IRCER" corresp="UNILIM">Institut de Recherche sur les CERamiques</idno>
            <idno type="stamp" n="IRCER-AXE3" corresp="IRCER">IRCER - Axe 3 : organisation structurale multiéchelle des matériaux</idno>
            <idno type="stamp" n="IMPEO" corresp="UNILIM">Institut Matériaux Procédés Environnement Ouvrages</idno>
            <idno type="stamp" n="TEST2-HALCNRS">TEST2-HALCNRS</idno>
          </seriesStmt>
          <notesStmt>
            <note type="audience" n="2">International</note>
            <note type="popular" n="0">No</note>
            <note type="peer" n="1">Yes</note>
          </notesStmt>
          <sourceDesc>
            <biblStruct>
              <analytic>
                <title xml:lang="en">Synthesis of 0.94 Na0.5Bi0.5TiO3 – 0.06 BaTiO3 (NBT-6BT) lead-free piezoelectric powder suitable for aerosol deposition (AD)</title>
                <author role="aut">
                  <persName>
                    <forename type="first">Innocent</forename>
                    <surname>Nomel</surname>
                  </persName>
                  <idno type="idhal" notation="numeric">807285</idno>
                  <idno type="halauthorid" notation="string">2213717-807285</idno>
                  <idno type="ORCID">https://orcid.org/0000-0003-4418-5927</idno>
                  <affiliation ref="#struct-1089379"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Jérôme</forename>
                    <surname>Lelievre</surname>
                  </persName>
                  <idno type="halauthorid">2478060-0</idno>
                  <affiliation ref="#struct-1089379"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Laurence</forename>
                    <surname>Boyer</surname>
                  </persName>
                  <idno type="halauthorid">651434-0</idno>
                  <affiliation ref="#struct-73554"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Olivier</forename>
                    <surname>Durand-Panteix</surname>
                  </persName>
                  <idno type="idhal" notation="numeric">773064</idno>
                  <idno type="halauthorid" notation="string">883641-773064</idno>
                  <idno type="ORCID">https://orcid.org/0000-0003-3926-0064</idno>
                  <affiliation ref="#struct-73554"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Pascal</forename>
                    <surname>Marchet</surname>
                  </persName>
                  <email type="md5">5f835411b89ba245df256cf246a6589c</email>
                  <email type="domain">unilim.fr</email>
                  <idno type="idhal" notation="string">pascal-marchet</idno>
                  <idno type="idhal" notation="numeric">1851</idno>
                  <idno type="halauthorid" notation="string">15707-1851</idno>
                  <idno type="ORCID">https://orcid.org/0000-0001-6694-6120</idno>
                  <idno type="IDREF">https://www.idref.fr/127468765</idno>
                  <idno type="VIAF">https://viaf.org/viaf/196193268</idno>
                  <idno type="ISNI">http://isni.org/isni/0000000138772469</idno>
                  <affiliation ref="#struct-522021"/>
                </author>
              </analytic>
              <monogr>
                <idno type="halJournalId" status="VALID">11588</idno>
                <idno type="issn">0272-8842</idno>
                <title level="j">Ceramics International</title>
                <imprint>
                  <publisher>Elsevier</publisher>
                  <biblScope unit="volume">48</biblScope>
                  <biblScope unit="issue">10</biblScope>
                  <biblScope unit="pp">14697-14707</biblScope>
                  <date type="datePub">2022</date>
                  <date type="dateEpub">2022-02-05</date>
                </imprint>
              </monogr>
              <idno type="doi">10.1016/j.ceramint.2022.02.005</idno>
            </biblStruct>
          </sourceDesc>
          <profileDesc>
            <langUsage>
              <language ident="en">English</language>
            </langUsage>
            <textClass>
              <keywords scheme="author">
                <term xml:lang="en">piezoelectric properties</term>
                <term xml:lang="en">perovskite</term>
                <term xml:lang="en">lead-free piezoelectric material</term>
              </keywords>
              <classCode scheme="halDomain" n="chim.mate">Chemical Sciences/Material chemistry</classCode>
              <classCode scheme="halTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halOldTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halTreeTypology" n="ART">Journal articles</classCode>
            </textClass>
            <abstract xml:lang="en">
              <p>The present work is devoted to the synthesis of 0.94 (Na0.5Bi0.5)TiO3-0.06 (BaTiO3) powders by solid-state reaction, suitable for Aerosol Deposition method (AD). The powders were synthetized using Na2CO3, Bi2O3, BaCO3 and TiO2. The raw powders were simultaneously milled / mixed by attrition milling in water. Two routes were studied, differing by the order of introduction of the raw materials, for three calcination temperatures. The first route (S1) led to the occurrence of Bi2Ti2O7 pyrochlore secondary phase. Attempts to suppress this phase by annealing were unsuccessful. The second route (S2) gave no secondary phase. The large grain size obtained at 950°C and 1050°C are not suitable for sintering or AD. However, the process carried out at 850°C resulted in powders suitable for both sintering and AD method. The ferroelectric and piezoelectric properties of the ceramic samples obtained using these powders are similar to the best-reported ones. Finally, we successfully used these powders for AD.</p>
            </abstract>
          </profileDesc>
        </biblFull>
      </listBibl>
    </body>
    <back>
      <listOrg type="structures">
        <org type="researchteam" xml:id="struct-1089379" status="VALID">
          <idno type="IdRef">223830259</idno>
          <idno type="RNSR">201722934J</idno>
          <orgName>IRCER - Axe 3 : organisation structurale multiéchelle des matériaux</orgName>
          <orgName type="acronym">IRCER-AXE3</orgName>
          <date type="start">2022-01-01</date>
          <desc>
            <address>
              <addrLine>Centre européen de la Céramique - 12 rue Atlantis 87068 LIMOGES CEDEX 3</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.ircer.fr/recherche/axe3</ref>
          </desc>
          <listRelation>
            <relation active="#struct-1089373" type="direct"/>
            <relation name="UMR7315" active="#struct-341038" type="indirect"/>
            <relation name="UMR7315" active="#struct-441569" type="indirect"/>
            <relation active="#struct-1088921" type="indirect"/>
            <relation active="#struct-5928" type="indirect"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-73554" status="VALID">
          <orgName>Centre de Transfert de Technologies Céramiques</orgName>
          <orgName type="acronym">CTTC</orgName>
          <desc>
            <address>
              <addrLine>Parc d'Ester - - Rue Soyouz - BP36823 - 87068 Limoges cedex</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.cttc.fr/index.php/accueil.html</ref>
          </desc>
          <listRelation>
            <relation active="#struct-366549" type="direct"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-522021" status="OLD">
          <idno type="IdRef">223830259</idno>
          <idno type="RNSR">201220198G</idno>
          <orgName>Institut de Recherche sur les CERamiques</orgName>
          <orgName type="acronym">IRCER</orgName>
          <date type="start">2018-01-01</date>
          <date type="end">2021-12-31</date>
          <desc>
            <address>
              <addrLine>Centre Européen de la Céramique, 12 Rue Atlantis, 87068 LIMOGES CEDEX</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.ircer.fr/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-301999" type="direct"/>
            <relation active="#struct-5928" type="indirect"/>
            <relation name="UMR7315" active="#struct-341038" type="direct"/>
            <relation name="UMR7315" active="#struct-441569" type="direct"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-1089373" status="VALID">
          <idno type="IdRef">223830259</idno>
          <idno type="ISNI">0000000404524960</idno>
          <idno type="RNSR">201220198G</idno>
          <idno type="ROR">https://ror.org/044qpwz88</idno>
          <idno type="Wikidata">Q30262390</idno>
          <orgName>Institut de Recherche sur les CERamiques</orgName>
          <orgName type="acronym">IRCER</orgName>
          <date type="start">2022-01-01</date>
          <desc>
            <address>
              <addrLine>Centre Européen de la Céramique, 12 Rue Atlantis, 87068 LIMOGES CEDEX</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.ircer.fr/</ref>
          </desc>
          <listRelation>
            <relation name="UMR7315" active="#struct-341038" type="direct"/>
            <relation name="UMR7315" active="#struct-441569" type="direct"/>
            <relation active="#struct-1088921" type="direct"/>
            <relation active="#struct-5928" type="indirect"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-341038" status="VALID">
          <idno type="IdRef">232435103</idno>
          <idno type="ISNI">000000010626358X</idno>
          <idno type="ROR">https://ror.org/02cte4b68</idno>
          <orgName>Institut de Chimie - CNRS Chimie</orgName>
          <orgName type="acronym">INC-CNRS</orgName>
          <date type="start">2009-10-01</date>
          <desc>
            <address>
              <addrLine>CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE3 rue Michel-Ange75794 PARIS CEDEX 16 - France</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.cnrs.fr/inc</ref>
          </desc>
        </org>
        <org type="regroupinstitution" xml:id="struct-441569" status="VALID">
          <idno type="IdRef">02636817X</idno>
          <idno type="ISNI">0000000122597504</idno>
          <idno type="ROR">https://ror.org/02feahw73</idno>
          <orgName>Centre National de la Recherche Scientifique</orgName>
          <orgName type="acronym">CNRS</orgName>
          <date type="start">1939-10-19</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.cnrs.fr/</ref>
          </desc>
        </org>
        <org type="regrouplaboratory" xml:id="struct-1088921" status="VALID">
          <idno type="IdRef">144784513</idno>
          <orgName>Institut Matériaux Procédés Environnement Ouvrages</orgName>
          <orgName type="acronym">IMPEO</orgName>
          <date type="start">2022-01-01</date>
          <desc>
            <address>
              <addrLine>Centre Européen de la Céramique12, rue Atlantis, parc d’Ester87068 Limoges Cedex</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.unilim.fr/recherche/laboratoires/ipmeo-actuel/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-5928" type="direct"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-5928" status="VALID">
          <idno type="IdRef">026403315</idno>
          <idno type="ISNI">0000000121654861</idno>
          <idno type="ROR">https://ror.org/02cp04407</idno>
          <orgName>Université de Limoges</orgName>
          <orgName type="acronym">UNILIM</orgName>
          <date type="start">1968-10-01</date>
          <desc>
            <address>
              <addrLine>33 rue François Mitterrand BP23204 87032 Limoges</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.unilim.fr</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-366549" status="INCOMING">
          <orgName>CTTC</orgName>
          <desc>
            <address>
              <country key="FR"/>
            </address>
          </desc>
        </org>
        <org type="regrouplaboratory" xml:id="struct-301999" status="VALID">
          <idno type="IdRef">144784513</idno>
          <orgName>Institut des Procédés Appliqués aux Matériaux</orgName>
          <orgName type="acronym">IPAM</orgName>
          <date type="end">2021-12-31</date>
          <desc>
            <address>
              <addrLine>Centre Européen de la Céramique12, rue Atlantis, parc d’Ester87068 Limoges Cedex</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.unilim.fr/recherche/laboratoires/ipam/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-5928" type="direct"/>
          </listRelation>
        </org>
      </listOrg>
    </back>
  </text>
</TEI>