<?xml version="1.0" encoding="utf-8"?>
<TEI xmlns="http://www.tei-c.org/ns/1.0" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:hal="http://hal.archives-ouvertes.fr/" xmlns:gml="http://www.opengis.net/gml/3.3/" xmlns:gmlce="http://www.opengis.net/gml/3.3/ce" version="1.1" xsi:schemaLocation="http://www.tei-c.org/ns/1.0 http://api.archives-ouvertes.fr/documents/aofr-sword.xsd">
  <teiHeader>
    <fileDesc>
      <titleStmt>
        <title>HAL TEI export of hal-03628271</title>
      </titleStmt>
      <publicationStmt>
        <distributor>CCSD</distributor>
        <availability status="restricted">
          <licence target="https://creativecommons.org/publicdomain/zero/1.0/">CC0 1.0 - Universal</licence>
        </availability>
        <date when="2026-05-02T14:06:52+02:00"/>
      </publicationStmt>
      <sourceDesc>
        <p part="N">HAL API Platform</p>
      </sourceDesc>
    </fileDesc>
  </teiHeader>
  <text>
    <body>
      <listBibl>
        <biblFull>
          <titleStmt>
            <title xml:lang="en">Development and validation according to the SANTE guidelines of a QuECh-ERS-UHPLC-QTOF-MS method for the screening of 204 pesticides in bivalves</title>
            <author role="aut">
              <persName>
                <forename type="first">Thierno</forename>
                <surname>Diallo</surname>
              </persName>
              <idno type="halauthorid">43170-0</idno>
              <affiliation ref="#struct-122685"/>
              <affiliation ref="#struct-154635"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Yassine</forename>
                <surname>Makni</surname>
              </persName>
              <email type="md5">6b7528684912925b4dcc69ea57a1ec7b</email>
              <email type="domain">anses.fr</email>
              <idno type="idhal" notation="numeric">1301621</idno>
              <idno type="halauthorid" notation="string">2533266-1301621</idno>
              <idno type="IDREF">https://www.idref.fr/272893269</idno>
              <idno type="ORCID">https://orcid.org/0009-0002-6697-8995</idno>
              <affiliation ref="#struct-122685"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Adélaïde</forename>
                <surname>Lerebours</surname>
              </persName>
              <idno type="halauthorid">1497050-0</idno>
              <affiliation ref="#struct-154635"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Hélène</forename>
                <surname>Thomas</surname>
              </persName>
              <idno type="halauthorid">670345-0</idno>
              <affiliation ref="#struct-154635"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Thierry</forename>
                <surname>Guérin</surname>
              </persName>
              <email type="md5">ed81801eefd76b2589494eb4d619d98b</email>
              <email type="domain">anses.fr</email>
              <idno type="idhal" notation="numeric">1174073</idno>
              <idno type="halauthorid" notation="string">646099-1174073</idno>
              <idno type="ORCID">https://orcid.org/0000-0003-4060-6616</idno>
              <idno type="IDREF">https://www.idref.fr/097657026</idno>
              <idno type="VIAF">https://viaf.org/viaf/214261236</idno>
              <affiliation ref="#struct-1063000"/>
            </author>
            <author role="crp">
              <persName>
                <forename type="first">Julien</forename>
                <surname>Parinet</surname>
              </persName>
              <email type="md5">9118df115397159e170978fe8ddc290c</email>
              <email type="domain">anses.fr</email>
              <idno type="idhal" notation="string">julien-parinet</idno>
              <idno type="idhal" notation="numeric">744279</idno>
              <idno type="halauthorid" notation="string">33203-744279</idno>
              <idno type="ORCID">https://orcid.org/0000-0003-0119-0929</idno>
              <idno type="ISNI">http://isni.org/isni/0000000301190929</idno>
              <idno type="IDREF">https://www.idref.fr/273083007</idno>
              <affiliation ref="#struct-122685"/>
            </author>
            <editor role="depositor">
              <persName>
                <forename>Adélaïde</forename>
                <surname>Lerebours</surname>
              </persName>
              <email type="md5">fe26324c44f3bf17dd5abdefd1189c6e</email>
              <email type="domain">gmail.com</email>
            </editor>
            <funder ref="#projanr-50988"/>
          </titleStmt>
          <editionStmt>
            <edition n="v1" type="current">
              <date type="whenSubmitted">2022-04-01 20:02:21</date>
              <date type="whenModified">2026-03-30 11:42:32</date>
              <date type="whenReleased">2022-04-05 08:57:16</date>
              <date type="whenProduced">2022</date>
              <date type="whenEndEmbargoed">2022-10-01</date>
              <ref type="file" target="https://hal.science/hal-03628271v1/document">
                <date notBefore="2022-10-01"/>
              </ref>
              <ref type="file" subtype="author" n="1" target="https://hal.science/hal-03628271v1/file/Diallo%20et%20al.%2C%202022.pdf" id="file-3628271-3172501">
                <date notBefore="2022-10-01"/>
              </ref>
            </edition>
            <respStmt>
              <resp>contributor</resp>
              <name key="686311">
                <persName>
                  <forename>Adélaïde</forename>
                  <surname>Lerebours</surname>
                </persName>
                <email type="md5">fe26324c44f3bf17dd5abdefd1189c6e</email>
                <email type="domain">gmail.com</email>
              </name>
            </respStmt>
          </editionStmt>
          <publicationStmt>
            <distributor>CCSD</distributor>
            <idno type="halId">hal-03628271</idno>
            <idno type="halUri">https://hal.science/hal-03628271</idno>
            <idno type="halBibtex">diallo:hal-03628271</idno>
            <idno type="halRefHtml">&lt;i&gt;Food Chemistry&lt;/i&gt;, 2022, 386, pp.132871. &lt;a target="_blank" href="https://dx.doi.org/10.1016/j.foodchem.2022.132871"&gt;&amp;#x27E8;10.1016/j.foodchem.2022.132871&amp;#x27E9;&lt;/a&gt;</idno>
            <idno type="halRef">Food Chemistry, 2022, 386, pp.132871. &amp;#x27E8;10.1016/j.foodchem.2022.132871&amp;#x27E9;</idno>
            <availability status="restricted">
              <licence target="https://about.hal.science/hal-authorisation-v1/">HAL Authorization<ref corresp="#file-3628271-3172501"/></licence>
            </availability>
          </publicationStmt>
          <seriesStmt>
            <idno type="stamp" n="INSU">INSU - Institut National des Sciences de l'Univers</idno>
            <idno type="stamp" n="ANSES">Agence nationale de sécurité sanitaire de l'alimentation, de l'environnement et du travail</idno>
            <idno type="stamp" n="CNRS">CNRS - Centre national de la recherche scientifique</idno>
            <idno type="stamp" n="AGREENIUM">Archive ouverte en agrobiosciences</idno>
            <idno type="stamp" n="UNIV-ROCHELLE">Université de La Rochelle</idno>
            <idno type="stamp" n="ANR">ANR</idno>
            <idno type="stamp" n="TEST3-HALCNRS">TEST3-HALCNRS</idno>
            <idno type="stamp" n="TEST4-HALCNRS">collection test</idno>
            <idno type="stamp" n="TEST5-HALCNRS">collection test 5</idno>
            <idno type="stamp" n="INEE-CNRS">Institut écologie et environnement du CNRS</idno>
            <idno type="stamp" n="LIENSS">LIttoral ENvironnement et Sociétés (LIENSs)</idno>
            <idno type="stamp" n="ANR-ONE-HEALTH">ANR-ONE-HEALTH</idno>
            <idno type="stamp" n="ANR-ONE-HEALTH-REF-ANR" corresp="ANR-ONE-HEALTH">ANR-ONE-HEALTH-REF-ANR</idno>
          </seriesStmt>
          <notesStmt>
            <note type="audience" n="2">International</note>
            <note type="popular" n="0">No</note>
            <note type="peer" n="1">Yes</note>
          </notesStmt>
          <sourceDesc>
            <biblStruct>
              <analytic>
                <title xml:lang="en">Development and validation according to the SANTE guidelines of a QuECh-ERS-UHPLC-QTOF-MS method for the screening of 204 pesticides in bivalves</title>
                <author role="aut">
                  <persName>
                    <forename type="first">Thierno</forename>
                    <surname>Diallo</surname>
                  </persName>
                  <idno type="halauthorid">43170-0</idno>
                  <affiliation ref="#struct-122685"/>
                  <affiliation ref="#struct-154635"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Yassine</forename>
                    <surname>Makni</surname>
                  </persName>
                  <email type="md5">6b7528684912925b4dcc69ea57a1ec7b</email>
                  <email type="domain">anses.fr</email>
                  <idno type="idhal" notation="numeric">1301621</idno>
                  <idno type="halauthorid" notation="string">2533266-1301621</idno>
                  <idno type="IDREF">https://www.idref.fr/272893269</idno>
                  <idno type="ORCID">https://orcid.org/0009-0002-6697-8995</idno>
                  <affiliation ref="#struct-122685"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Adélaïde</forename>
                    <surname>Lerebours</surname>
                  </persName>
                  <idno type="halauthorid">1497050-0</idno>
                  <affiliation ref="#struct-154635"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Hélène</forename>
                    <surname>Thomas</surname>
                  </persName>
                  <idno type="halauthorid">670345-0</idno>
                  <affiliation ref="#struct-154635"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Thierry</forename>
                    <surname>Guérin</surname>
                  </persName>
                  <email type="md5">ed81801eefd76b2589494eb4d619d98b</email>
                  <email type="domain">anses.fr</email>
                  <idno type="idhal" notation="numeric">1174073</idno>
                  <idno type="halauthorid" notation="string">646099-1174073</idno>
                  <idno type="ORCID">https://orcid.org/0000-0003-4060-6616</idno>
                  <idno type="IDREF">https://www.idref.fr/097657026</idno>
                  <idno type="VIAF">https://viaf.org/viaf/214261236</idno>
                  <affiliation ref="#struct-1063000"/>
                </author>
                <author role="crp">
                  <persName>
                    <forename type="first">Julien</forename>
                    <surname>Parinet</surname>
                  </persName>
                  <email type="md5">9118df115397159e170978fe8ddc290c</email>
                  <email type="domain">anses.fr</email>
                  <idno type="idhal" notation="string">julien-parinet</idno>
                  <idno type="idhal" notation="numeric">744279</idno>
                  <idno type="halauthorid" notation="string">33203-744279</idno>
                  <idno type="ORCID">https://orcid.org/0000-0003-0119-0929</idno>
                  <idno type="ISNI">http://isni.org/isni/0000000301190929</idno>
                  <idno type="IDREF">https://www.idref.fr/273083007</idno>
                  <affiliation ref="#struct-122685"/>
                </author>
              </analytic>
              <monogr>
                <idno type="halJournalId" status="VALID">13403</idno>
                <idno type="issn">0308-8146</idno>
                <idno type="eissn">1873-7072</idno>
                <title level="j">Food Chemistry</title>
                <imprint>
                  <publisher>Elsevier</publisher>
                  <biblScope unit="volume">386</biblScope>
                  <biblScope unit="pp">132871</biblScope>
                  <date type="datePub">2022</date>
                  <date type="dateEpub">2022-03-31</date>
                </imprint>
              </monogr>
              <idno type="doi">10.1016/j.foodchem.2022.132871</idno>
              <idno type="pubmed">35381542</idno>
              <ref target="https://ars.els-cdn.com/content/image/1-s2.0-S0308814622008330-mmc1.docx" type="seeAlso"/>
              <ref type="publisher">https://www.sciencedirect.com/science/article/pii/S0308814622008330</ref>
            </biblStruct>
          </sourceDesc>
          <profileDesc>
            <langUsage>
              <language ident="en">English</language>
            </langUsage>
            <textClass>
              <keywords scheme="author">
                <term xml:lang="en">QuEChERS</term>
                <term xml:lang="en">Taguchi Orthogonal Array</term>
                <term xml:lang="en">Bivalves</term>
                <term xml:lang="en">Pesticides</term>
                <term xml:lang="en">LC-HRMS acquisition modes</term>
                <term xml:lang="en">Qualitative screening</term>
              </keywords>
              <classCode scheme="mesh">Bivalvia</classCode>
              <classCode scheme="mesh">Mass Spectrometry</classCode>
              <classCode scheme="mesh">Pesticides</classCode>
              <classCode scheme="halDomain" n="chim.anal">Chemical Sciences/Analytical chemistry</classCode>
              <classCode scheme="halDomain" n="sdv.ida">Life Sciences [q-bio]/Food engineering</classCode>
              <classCode scheme="halDomain" n="sdv.tox">Life Sciences [q-bio]/Toxicology</classCode>
              <classCode scheme="halTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halOldTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halTreeTypology" n="ART">Journal articles</classCode>
            </textClass>
            <abstract xml:lang="en">
              <p>A qualitative screening high resolution mass spectrometry method was developed and validated according to the EU SANTE/12682/2019 guidelines for the analysis of 204 pesticides in seven commercial bivalve species spiked at three concentrations (0.01, 0.05 and, 0.1 mg.kg−1). Samples were extracted using QuEChERS and analysed using ultra-high-performance liquid chromatography coupled to quadrupole time-of-flight mass spectrometry. The QuEChERS method was optimised by the Taguchi Orthogonal Array approach. The best conditions were obtained with pure ACN, MgSO4/NaCl as extraction salts, MgSO4/PSA/C18 as clean-up, and the non-dilution of extracts. The impact of different HRMS acquisition modes on detection and identification rates were also evaluated. The screening detection limits were determined to be 0.01 mg.kg−1 and 0.1 for 66% and 87% of pesticides, respectively. These screening procedure was finally applied to different bivalve samples using target and suspect analysis. This allowed the identification of diuron and its metabolite 1-(3,4-dichlorophenyl)-3-methylurea in the investigated samples</p>
            </abstract>
          </profileDesc>
        </biblFull>
      </listBibl>
    </body>
    <back>
      <listOrg type="structures">
        <org type="laboratory" xml:id="struct-122685" status="OLD">
          <idno type="RNSR">201023301N</idno>
          <orgName>Laboratoire de sécurité des aliments de Maisons-Alfort</orgName>
          <orgName type="acronym">LSAl</orgName>
          <date type="start">2010-07-01</date>
          <date type="end">2013-02-21</date>
          <desc>
            <address>
              <addrLine>14, rue Pierre et Marie Curie 94701 Maisons-Alfort Cedex</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.anses.fr/</ref>
          </desc>
          <listRelation>
            <relation active="#struct-301715" type="direct"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-154635" status="VALID">
          <idno type="IdRef">184240557</idno>
          <idno type="ISNI">000000040385903X</idno>
          <idno type="RNSR">201220407J</idno>
          <idno type="ROR">https://ror.org/00r8amq78</idno>
          <orgName>LIttoral ENvironnement et Sociétés</orgName>
          <orgName type="acronym">LIENSs</orgName>
          <date type="start">2012-01-01</date>
          <desc>
            <address>
              <addrLine>Institut du Littoral et de l'Environnement, 2 rue Olympe de Gouges 17 000 La Rochelle - France</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://lienss.univ-larochelle.fr/</ref>
          </desc>
          <listRelation>
            <relation name="UMR7266" active="#struct-300045" type="direct"/>
            <relation active="#struct-300311" type="direct"/>
            <relation name="UMR7266" active="#struct-441569" type="direct"/>
          </listRelation>
        </org>
        <org type="department" xml:id="struct-1063000" status="VALID">
          <orgName>Direction de la Stratégie et des Programmes</orgName>
          <orgName type="acronym">DSP</orgName>
          <date type="start">2020-07-01</date>
          <desc>
            <address>
              <addrLine>ANSES14 rue Pierre et Marie Curie94701 MAISONS-ALFORT Cedex</addrLine>
              <country key="FR"/>
            </address>
          </desc>
          <listRelation>
            <relation active="#struct-301715" type="direct"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-301715" status="VALID">
          <idno type="IdRef">148269761</idno>
          <idno type="ISNI">0000 0001 0584 7022</idno>
          <idno type="ROR">https://ror.org/0471kz689</idno>
          <idno type="Wikidata">Q392520</idno>
          <orgName>Agence nationale de sécurité sanitaire de l'alimentation, de l'environnement et du travail</orgName>
          <orgName type="acronym">ANSES</orgName>
          <date type="start">2010-07-01</date>
          <desc>
            <address>
              <addrLine>14 rue Pierre et Marie Curie94701 MAISONS-ALFORT Cedex</addrLine>
              <country key="FR"/>
            </address>
          </desc>
        </org>
        <org type="institution" xml:id="struct-300045" status="VALID">
          <idno type="IdRef">029349265</idno>
          <idno type="ISNI">0000 0001 2154 1736</idno>
          <idno type="ROR">https://ror.org/04kdfz702</idno>
          <idno type="Wikidata">Q3152437</idno>
          <orgName>Institut national des sciences de l'Univers</orgName>
          <orgName type="acronym">INSU - CNRS</orgName>
          <date type="start">2007-04-19</date>
          <desc>
            <address>
              <addrLine>INSU-CNRS3 rue Michel-Ange, 75794 Paris Cedex 16</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.insu.cnrs.fr</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-300311" status="VALID">
          <idno type="IdRef">035375043</idno>
          <idno type="ISNI">0000 0001 2169 7335</idno>
          <idno type="ROR">https://ror.org/04mv1z119</idno>
          <orgName>La Rochelle Université</orgName>
          <orgName type="acronym">ULR</orgName>
          <desc>
            <address>
              <addrLine>Technoforum - 23 avenue Albert Einstein - BP 33060 - 17031 La Rochelle - France</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.univ-larochelle.fr</ref>
          </desc>
        </org>
        <org type="regroupinstitution" xml:id="struct-441569" status="VALID">
          <idno type="IdRef">02636817X</idno>
          <idno type="ISNI">0000000122597504</idno>
          <idno type="ROR">https://ror.org/02feahw73</idno>
          <orgName>Centre National de la Recherche Scientifique</orgName>
          <orgName type="acronym">CNRS</orgName>
          <date type="start">1939-10-19</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.cnrs.fr/</ref>
          </desc>
        </org>
      </listOrg>
      <listOrg type="projects">
        <org type="anrProject" xml:id="projanr-50988" status="VALID">
          <idno type="anr">ANR-19-CE21-0002</idno>
          <orgName>AlimOmic</orgName>
          <desc>Traquer les Pesticides Présents dans l'Alimentation par l'Emploi de la Spectrométrie de Masse Haute Résolution : approche ciblée et non-ciblée</desc>
          <date type="start">2019</date>
        </org>
      </listOrg>
    </back>
  </text>
</TEI>