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            <funder>We thank the Department of Science and Technology (DST), India; the CNRS, Université de Rennes 1, the European Commission through the ERC-CoG 725184 MULTIPROSMM (Project No. 725184) for financial support, and also support for the Single Crystal CCD X-ray Diffractometer facility at IIT-Kanpur. V.C. is grateful to the DST for a J. C. Bose fellowship. P.K. and A.S. thank the University Grants Commission (UGC), India for Senior Research Fellowships. G.R. acknowledges DST/SERB for funding (Nos. CRG/2018/000430, DST/SJF/CSA-03/2018-10, SB/SJF/2019-20/12). We sincerely thank Mr. Prakash Nayak, NISER, Bhubanswar, Odisha, India, for the PXRD measurements.</funder>
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                <term xml:lang="en">Lanthanides</term>
                <term xml:lang="en">Magnetic properties</term>
                <term xml:lang="en">Ions</term>
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              <p>A series of homometallic dinuclear lanthanide complexes containing nonequivalent lanthanide metal centers [Ln(LH)(LH)(CHOH)(N)]MeOHHO [, Ln = Dy,  = 0,  = 2; , Ln = Tb,  = 1,  = 1] have been synthesized [LH = 6-((bis(2-hydroxyethyl)amino)-'-(2-hydroxybenzylidene)picolinohydrazide] and characterized. The dinuclear assembly contains two different types of nine-coordinated lanthanide centers, because the nonequivalent binding of the azide co-ligand as well as the varying coordination of the deprotonated Schiff base ligand. Detailed magnetic studies have been performed on the complexes  and . Complex  and its diluted analogue () are zero-field SMMs with effective energy barriers () of magnetization reversal equal to 59(3) K and 66(3) K and relaxation times of τ = 10(4) × 10 s and 10(4) × 10 s, respectively. On the other hand, complex  shows a field-induced SMM behavior. Combined  and density functional theory calculations were performed to explain the experimental findings and to unravel the nature of the magnetic anisotropy, exchange-coupled spectra, and magnetic exchange interactions between the two lanthanide centers.</p>
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