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            <title xml:lang="fr">Optimisation des prélèvements par accumulation et dosage par couplage GC/MS des COV présents dans les stockages d'ordures ménagères</title>
            <title xml:lang="fr" type="sub">Première approche de comparaison de méthodes analytiques</title>
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                <forename type="first">Rodica</forename>
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            <idno type="halRefHtml">&lt;i&gt;Environnement, Ingénierie &amp; Développement&lt;/i&gt;, 2004, N°33 - 1er Trimestre 2004, pp.34-44. &lt;a target="_blank" href="https://dx.doi.org/10.4267/dechets-sciences-techniques.2069"&gt;&amp;#x27E8;10.4267/dechets-sciences-techniques.2069&amp;#x27E9;&lt;/a&gt;</idno>
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                <title xml:lang="fr">Optimisation des prélèvements par accumulation et dosage par couplage GC/MS des COV présents dans les stockages d'ordures ménagères</title>
                <title xml:lang="fr" type="sub">Première approche de comparaison de méthodes analytiques</title>
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                    <forename type="first">Rodica</forename>
                    <surname>Chiriac</surname>
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              <p>The present article is devoted to an approach of optimization of required conditions to traces VOCs analysis coming from household wastes stocked in specially designed pilots for studying maturation. A known volume of the gas phase goes through tubes filled with various adsorbents like Tenax, Chromosorb, Tenax-graphitized carbon and active charcoal. To extract VOCs, thermal desorption has been used for the first three adsorbents while CS2 extraction has been applied on active charcoal tubes. About 200 VOCs were surely identified and performances of the two sample preparation processes were compared: accumulation followed by thermal desorption or followed by solvent extraction. Both analysis techniques are compared in order to set all the precautions for a reliable quantitative analysis.</p>
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              <p>Le travail présenté constitue une approche de l'optimisation des conditions nécessaires à l'analyse des composés organiques volatils (COV) émis par des ordures ménagères en cours de maturation dans un pilote. Un volume connu de la phase gaz du pilote parcourt des tubes à accumulation de différentes natures : Tenax, Chromosorb, Tenax-carbone graphite et charbon actif. Les COV piégés sur les trois premiers types de tubes ont été extraits pas désorption thermique et par extraction au sulfure de carbone pour les tubes à charbon actif. Plus de 200 COV sont identifiés avec certitude et les performances des deux filières accumulation/désorption thermique et accumulation/extraction par solvant sont comparées. Quelques précautions à prendre pour un dosage quantitatif fiable sont émises.</p>
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