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            <funder>RCK grateful acknowledges the financial support of AVRUL (Agence pour la Valorisation de la Recherche Universitaire du Limousin) for his stay in IRCER, UMRCNRS 7315, Limoges, France under 2018 AVRUL postgraduate internship. The authors also like to express gratitude to the Director of IRCER for having made accessible all accommodations for carrying out this work in the laboratory. This project also received the contribution of the FLAIR Fellowship African Academic of Science and the Royal Society through the funding N° FLR/R1/201402. The participation of ASY and JLP has been supported by EPSRC through grant EP/T013524/1.</funder>
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                <term xml:lang="en">Laterite</term>
                <term xml:lang="en">Sodium silicate</term>
                <term xml:lang="en">Phosphoric acid</term>
                <term xml:lang="en">Inorganic polymer cement</term>
                <term xml:lang="en">Mechanical properties</term>
                <term xml:lang="en">Electron paramagnetic resonance</term>
                <term xml:lang="en">57Fe Mössbauer spectroscopy</term>
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              <p>In this work, two different laterites (iron contents of 13.07 and 49.34 wt%, respectively, for lateritic clay, LAC, and iron-rich laterite, LAI) were selected and calcined at 600 °C. The obtained calcined laterites, namely LAI600 and LAC600, were separately mixed with an alkaline solution (silicate modulus of 1.35) or an acidic solution (phosphoric acid solution at pH ≤ 2) for the synthesis of inorganic polymer products. The fabricated products were cured at 20 °C (ambient) and 40 °C (oven). The obtained results showed that the compressive strength of each series of alkaline-based inorganic polymer binder increased with ageing time (7 and 28 days) for room temperature curing, while the reverse trend was noted for oven-cured specimens. The best mechanical performance was obtained when using a phosphoric acid solution, 38 and 52 ± 1 MPa; 62 and 65 ± 1 MPa at 28 days for LAC and LAI respectively. It appeared that a higher iron content within the laterite contributed to an increase in the compressive strength under acidic conditions (LAI (59 MPa) &amp;gt; LAC (48 MPa)) compared to the behavior obtained under alkaline conditions (LAI (6 MPa) &amp;lt; LAC (29 MPa)). Accordingly, the acidic products exhibited a dense structure (with lower porosity) and contained amorphous iron/aluminium phosphate phases such as berlinite (FePO4), iron hydrogen phosphate hydrate (Fe3H15(PO4)8·4H2O), ferrowyllieite (AlFe2Na2(PO4)3) and sodium iron phosphate (Na3Fe2(PO4)3) arising from the alteration of iron minerals in an acidic medium, confirmed by Mössbauer spectroscopy and electron paramagnetic resonance spectroscopy.</p>
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