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              <p>The use of contactless magnetic forces meets numerous needs in microelectromechanical systems (MEMS) or microfluidic devices. In this view, heterogeneous materials integrating magnetic nanostructures within a non-magnetic matrix such as polymer can produce local variations of magnetic field, at the sub-micrometer scale. Here we report on the synthesis of magnetic composites using electrospun nanofilaments and a polydimethylsiloxane (PDMS) matrix. Varying the precursor nature and heat treatment conditions, we obtained single phase filaments of Fe, FeNi, and MFe&lt;sub&gt;2&lt;/sub&gt;O&lt;sub&gt;4&lt;/sub&gt; (M = Co, Fe, Ni). Thanks to a fine investigation of their structure and morphology, it was possible to measure from magnetically-soft (µ&lt;sub&gt;0&lt;/sub&gt;H&lt;sub&gt;C&lt;/sub&gt; ≤ 5 mT) to relatively hard (µ&lt;sub&gt;0&lt;/sub&gt;H&lt;sub&gt;C&lt;/sub&gt; up to 93 mT, M&lt;sub&gt;R&lt;/sub&gt;/M&lt;sub&gt;S&lt;/sub&gt; up to 0.5) behaviors. The common one-dimensional shape of these filaments leads to an anisotropic magnetic response. This can be exploited to achieve self-organization of the filaments in arrays within the non-magnetic matrix. We show the first step towards the development of magnetically anisotropic membranes of PDMS with 0.23 wt% Fe filaments. These composite materials are promising for implementing magnetic functions in microsystems while circumventing complex micro-fabrication steps.</p>
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