Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths - Archive ouverte HAL
Article Dans Une Revue Chemical Communications Année : 2017

Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Katharina Märker
Gaël de Paëpe

Résumé

2D double-quantum single-quantum correlation spectra with arbitrary spectral widths can be recorded with SR26 and related supercycled recoupling sequences when applying Supercycle-Timing-Compensation (STiC) phase shifts. This concept widely extends the applicability of supercycled sequences, most importantly for obtaining long-range distance constraints for structure determination with solid-state NMR.
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Dates et versions

hal-02048398 , version 1 (28-09-2021)

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Citer

Katharina Märker, Sabine Hediger, Gaël de Paëpe. Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths. Chemical Communications, 2017, 53 (65), pp.9155-9158. ⟨10.1039/C7CC04890D⟩. ⟨hal-02048398⟩
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