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                <term xml:lang="en"> Epitaxial growth</term>
                <term xml:lang="en"> Epitaxial thin films</term>
                <term xml:lang="en"> Exchange bias</term>
                <term xml:lang="en"> Lanthanum compounds</term>
                <term xml:lang="en"> Single crystal substrates</term>
                <term xml:lang="en"> Nonferromagnetic layers</term>
                <term xml:lang="en"> Theoretical calculations</term>
                <term xml:lang="en"> Strain engineering</term>
                <term xml:lang="en">Electron holography</term>
                <term xml:lang="en"> Ground state</term>
                <term xml:lang="en"> Holography</term>
                <term xml:lang="en"> Phase segregations</term>
                <term xml:lang="en"> Manganese oxide</term>
                <term xml:lang="en"> Manganites</term>
                <term xml:lang="en"> Phase separation</term>
                <term xml:lang="en"> Single crystals</term>
                <term xml:lang="en"> Surface segregation</term>
                <term xml:lang="en"> Thin films</term>
                <term xml:lang="en"> Different substrates</term>
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              <p>Epitaxial strain alters the physical properties of thin films grown on single crystal substrates. Thin film oxides are particularly apt for strain engineering new functionalities in ferroic materials. In the case of La2/3Ca1/3MnO3 (LCMO) thin films, here we show the first experimental images obtained by electron holography demonstrating that epitaxial strain induces the segregation of a flat and uniform nonferromagnetic layer with antiferromagnetic (AFM) character at the top surface of a ferromagnetic (FM) layer, the whole film being chemical and structurally homogeneous at room temperature. For different substrates and growth conditions the tetragonality of LCMO at room temperature, defined as τ = |c - a|/a, is the driving force for a phase coexistence above an approximate critical value of τC ≈ 0.024. Theoretical calculations prove that the increased tetragonality changes the energy balance of the FM and AFM ground states in strained LCMO, enabling the formation of magnetically inhomogeneous states. This work gives the key evidence that opens a new route to synthesize strain-induced exchanged-biased FM-AFM bilayers in single thin films, which could serve as building blocks of future spintronic devices.</p>
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