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Article Dans Une Revue Journal of Thermal Analysis and Calorimetry Année : 2013

TG–DSC–FTIR–MS study of gaseous compounds evolved during thermal decomposition of styrene-butadiene rubber

Résumé

The thermal decomposition behavior of styrene-butadiene rubber was studied using a system equipped with thermogravimetric analysis, differential thermal analysis, Fourier transform infrared spectroscopy, and mass spectroscopy. Two different experiments were conducted. From these experiments, thermogravimetric analysis results indicated a mass loss of 58 % in the temperature range of ~290–480 °C and a mass loss of 39 % in the temperature range beyond 600 °C. Scanning electron microscopy coupled with energy-dispersive X-ray spectroscopy confirmed the presence of oxides, even at 1,000 °C, accounting for the Zn, Mg, Al, Si, and Ca in the original sample.

Dates et versions

hal-01713108 , version 1 (20-02-2018)

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Citer

Antonyraj Arockiasamy, Hossein Toghiani, David Oglesby, Mark F. Horstemeyer, Jean-Luc Bouvard, et al.. TG–DSC–FTIR–MS study of gaseous compounds evolved during thermal decomposition of styrene-butadiene rubber. Journal of Thermal Analysis and Calorimetry, 2013, 111 (1), pp.535 - 542. ⟨10.1007/s10973-012-2559-0⟩. ⟨hal-01713108⟩
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