Evaluation of morphological representative sample sizes for nanolayered polymer blends - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Journal of Microscopy Année : 2016

Evaluation of morphological representative sample sizes for nanolayered polymer blends

Résumé

The size of representative microstructural samples obtained from atomic force microscopy is addressed in this paper. The case of an archetypal one-dimensional nanolayered polymer blend is considered. Image analysis is performed on micrographs obtained through atomic force microscopy, yielding statistical data concerning morphological properties of the material. The variability in terms of microstructural morphology is due to the thermomechanical processing route. The statistical data is used in order to estimate sample size representativity, based on an asymptotic relationship relating the inherent point variance of the indicator function of one material phase to the statistical, size-dependent, ensemble variance of the same function. From the study of nanolayered material systems, the statistical approach was found to be an effective mean for discriminating and characterizing multiple scales of heterogeneity.
Fichier principal
Vignette du fichier
PIMM_JMI_Dirrenberger_2016.pdf (1.17 Mo) Télécharger le fichier
Origine : Fichiers produits par l'(les) auteur(s)
Loading...

Dates et versions

hal-01383497 , version 1 (18-10-2016)

Identifiants

  • HAL Id : hal-01383497 , version 1
  • DOI : 10.1111/jmi.12415
  • ENSAM : http://hdl.handle.net/10985/11276

Citer

Adrien Bironeau, Justin Dirrenberger, Cyrille Sollogoub, Guillaume Miquelard-Garnier, Sébastien Roland. Evaluation of morphological representative sample sizes for nanolayered polymer blends. Journal of Microscopy, 2016, 264 (1), pp.48-58. ⟨10.1111/jmi.12415⟩. ⟨hal-01383497⟩
202 Consultations
116 Téléchargements

Altmetric

Partager

Gmail Facebook X LinkedIn More