<?xml version="1.0" encoding="utf-8"?>
<TEI xmlns="http://www.tei-c.org/ns/1.0" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:hal="http://hal.archives-ouvertes.fr/" xmlns:gml="http://www.opengis.net/gml/3.3/" xmlns:gmlce="http://www.opengis.net/gml/3.3/ce" version="1.1" xsi:schemaLocation="http://www.tei-c.org/ns/1.0 http://api.archives-ouvertes.fr/documents/aofr-sword.xsd">
  <teiHeader>
    <fileDesc>
      <titleStmt>
        <title>HAL TEI export of hal-01173918</title>
      </titleStmt>
      <publicationStmt>
        <distributor>CCSD</distributor>
        <availability status="restricted">
          <licence target="https://creativecommons.org/publicdomain/zero/1.0/">CC0 1.0 - Universal</licence>
        </availability>
        <date when="2026-05-19T15:25:54+02:00"/>
      </publicationStmt>
      <sourceDesc>
        <p part="N">HAL API Platform</p>
      </sourceDesc>
    </fileDesc>
  </teiHeader>
  <text>
    <body>
      <listBibl>
        <biblFull>
          <titleStmt>
            <title xml:lang="en">Isolation and characterization of cellulose nanocrystals from industrial by-products of Agave tequilana and barley</title>
            <author role="aut">
              <persName>
                <forename type="first">Etzael</forename>
                <surname>Espino-Perez</surname>
              </persName>
              <idno type="halauthorid">924865-0</idno>
              <affiliation ref="#struct-135725"/>
              <affiliation ref="#struct-703"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Mélissa</forename>
                <surname>Cakir</surname>
              </persName>
              <idno type="halauthorid">924890-0</idno>
              <affiliation ref="#struct-703"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Sandra</forename>
                <surname>Domenek</surname>
              </persName>
              <email type="md5">f3722ab9ae20f868d58b5c5499feb8cb</email>
              <email type="domain">agroparistech.fr</email>
              <idno type="idhal" notation="string">sandra-domenek</idno>
              <idno type="idhal" notation="numeric">180562</idno>
              <idno type="halauthorid" notation="string">22411-180562</idno>
              <idno type="RESEARCHERID">http://www.researcherid.com/rid/C-8095-2015</idno>
              <idno type="ORCID">https://orcid.org/0000-0003-3012-041X</idno>
              <idno type="IDREF">https://www.idref.fr/088785254</idno>
              <idno type="RESEARCHERID">http://www.researcherid.com/rid/http://www.researcherid.com/rid/C-8095-2015</idno>
              <affiliation ref="#struct-135725"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Alma Delia</forename>
                <surname>Román-Gutiérrez</surname>
              </persName>
              <idno type="halauthorid">924891-0</idno>
              <affiliation ref="#struct-424145"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Naceur</forename>
                <surname>Belgacem</surname>
              </persName>
              <email type="md5">c91d9850f12edf0693b33f5920be1238</email>
              <email type="domain">efpg.inpg.fr</email>
              <idno type="idhal" notation="string">mohamed-naceur-belgacem</idno>
              <idno type="idhal" notation="numeric">1253655</idno>
              <idno type="halauthorid" notation="string">924888-1253655</idno>
              <idno type="ORCID">https://orcid.org/0000-0002-3317-7369</idno>
              <idno type="ISNI">http://isni.org/isni/0000000384814492</idno>
              <idno type="VIAF">https://viaf.org/viaf/59170858294407681389</idno>
              <idno type="RESEARCHERID">http://www.researcherid.com/rid/B-7123-2016</idno>
              <idno type="GOOGLE SCHOLAR">https://scholar.google.fr/citations?user=1wGsMNsAAAAJ</idno>
              <idno type="IDREF">https://www.idref.fr/084755202</idno>
              <idno type="RESEARCHERID">http://www.researcherid.com/rid/http://www.researcherid.com/rid/B-7123-2016</idno>
              <affiliation ref="#struct-703"/>
              <affiliation ref="#struct-703"/>
            </author>
            <author role="aut">
              <persName>
                <forename type="first">Julien</forename>
                <surname>Bras</surname>
              </persName>
              <email type="md5">ea0a89e6b694a3c781e952cb707ad227</email>
              <email type="domain">grenoble-inp.frFundingAgencyandGrantNumberInstitut</email>
              <idno type="idhal" notation="numeric">1070286</idno>
              <idno type="halauthorid" notation="string">320877-1070286</idno>
              <affiliation ref="#struct-703"/>
              <affiliation ref="#struct-703"/>
            </author>
            <editor role="depositor">
              <persName>
                <forename>Archive Ouverte</forename>
                <surname>ProdInra</surname>
              </persName>
              <email type="md5">9e5ed7d56b52b3d4383123b1ffb42236</email>
              <email type="domain">inrae.fr</email>
            </editor>
            <funder ref="#projanr-37552"/>
            <funder>Mexican Scholarship Council (CONACyT)  (213840) ; LGP2 is part of the LabEx Tec 21 (Investissements d'Avenir)  (ANR-11-LABX-0030) ; Energies du Futur and PolyNat Carnot Institutes (Investissements d'Avenir) ( ANR-11-CARN-007-01)  (ANR-11-CARN-030-01 )</funder>
          </titleStmt>
          <editionStmt>
            <edition n="v1" type="current">
              <date type="whenSubmitted">2025-07-25 17:44:22</date>
              <date type="whenModified">2025-09-27 19:05:51</date>
              <date type="whenReleased">2015-07-07 21:17:50</date>
              <date type="whenProduced">2014</date>
              <ref type="externalLink" target="https://api.istex.fr/ark:/67375/6H6-SMR46TX2-X/fulltext.pdf?sid=hal"/>
              <fs>
                <f name="inra_etatDocument_local" notation="string" n="VE">
                  <string>inra_etatDocument_local_VE</string>
                </f>
                <f name="inra_publicVise_local" notation="string" n="SC">
                  <string>inra_publicVise_local_SC</string>
                </f>
              </fs>
            </edition>
            <respStmt>
              <resp>contributor</resp>
              <name key="132775">
                <persName>
                  <forename>Archive Ouverte</forename>
                  <surname>ProdInra</surname>
                </persName>
                <email type="md5">9e5ed7d56b52b3d4383123b1ffb42236</email>
                <email type="domain">inrae.fr</email>
              </name>
            </respStmt>
          </editionStmt>
          <publicationStmt>
            <distributor>CCSD</distributor>
            <idno type="halId">hal-01173918</idno>
            <idno type="halUri">https://hal.science/hal-01173918</idno>
            <idno type="halBibtex">espinoperez:hal-01173918</idno>
            <idno type="halRefHtml">&lt;i&gt;Industrial Crops and Products&lt;/i&gt;, 2014, 62, pp.552-559. &lt;a target="_blank" href="https://dx.doi.org/10.1016/j.indcrop.2014.09.017"&gt;&amp;#x27E8;10.1016/j.indcrop.2014.09.017&amp;#x27E9;&lt;/a&gt;</idno>
            <idno type="halRef">Industrial Crops and Products, 2014, 62, pp.552-559. &amp;#x27E8;10.1016/j.indcrop.2014.09.017&amp;#x27E9;</idno>
            <availability status="restricted"/>
          </publicationStmt>
          <seriesStmt>
            <idno type="stamp" n="AGROPARISTECH">AgroParisTech</idno>
            <idno type="stamp" n="UGA">HAL Grenoble Alpes</idno>
            <idno type="stamp" n="CNRS">CNRS - Centre national de la recherche scientifique</idno>
            <idno type="stamp" n="CNAM">Conservatoire National des Arts et Métiers</idno>
            <idno type="stamp" n="INPG">Institut polytechnique de Grenoble</idno>
            <idno type="stamp" n="INRA">INRA - Institut national de la recherche agronomique</idno>
            <idno type="stamp" n="LGP2">Laboratoire Génie des procédés papetiers</idno>
            <idno type="stamp" n="GENIAL">GENIAL</idno>
            <idno type="stamp" n="AGREENIUM">Archive ouverte en agrobiosciences</idno>
            <idno type="stamp" n="AGROPARISTECH-ORG">AgroParisTech-ORG</idno>
            <idno type="stamp" n="AGROPARISTECH-SPAB" corresp="AGROPARISTECH-ORG">AgroParisTech-SPAB</idno>
            <idno type="stamp" n="APT_SP">APT_SP</idno>
            <idno type="stamp" n="INRAE">Institut National de Recherche en Agriculture, Alimentation et Environnement</idno>
            <idno type="stamp" n="ANR">ANR</idno>
            <idno type="stamp" n="TEST3-HALCNRS">TEST3-HALCNRS</idno>
            <idno type="stamp" n="HESAM-CNAM" corresp="HESAM">Conservatoire National des Arts et Métiers - Hesam</idno>
            <idno type="stamp" n="HESAM">Hesam</idno>
            <idno type="stamp" n="TEST-UGA">TEST-UGA</idno>
          </seriesStmt>
          <notesStmt>
            <note type="audience" n="1">Not set</note>
            <note type="popular" n="0">No</note>
            <note type="peer" n="1">Yes</note>
          </notesStmt>
          <sourceDesc>
            <biblStruct>
              <analytic>
                <title xml:lang="en">Isolation and characterization of cellulose nanocrystals from industrial by-products of Agave tequilana and barley</title>
                <author role="aut">
                  <persName>
                    <forename type="first">Etzael</forename>
                    <surname>Espino-Perez</surname>
                  </persName>
                  <idno type="halauthorid">924865-0</idno>
                  <affiliation ref="#struct-135725"/>
                  <affiliation ref="#struct-703"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Mélissa</forename>
                    <surname>Cakir</surname>
                  </persName>
                  <idno type="halauthorid">924890-0</idno>
                  <affiliation ref="#struct-703"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Sandra</forename>
                    <surname>Domenek</surname>
                  </persName>
                  <email type="md5">f3722ab9ae20f868d58b5c5499feb8cb</email>
                  <email type="domain">agroparistech.fr</email>
                  <idno type="idhal" notation="string">sandra-domenek</idno>
                  <idno type="idhal" notation="numeric">180562</idno>
                  <idno type="halauthorid" notation="string">22411-180562</idno>
                  <idno type="RESEARCHERID">http://www.researcherid.com/rid/C-8095-2015</idno>
                  <idno type="ORCID">https://orcid.org/0000-0003-3012-041X</idno>
                  <idno type="IDREF">https://www.idref.fr/088785254</idno>
                  <idno type="RESEARCHERID">http://www.researcherid.com/rid/http://www.researcherid.com/rid/C-8095-2015</idno>
                  <affiliation ref="#struct-135725"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Alma Delia</forename>
                    <surname>Román-Gutiérrez</surname>
                  </persName>
                  <idno type="halauthorid">924891-0</idno>
                  <affiliation ref="#struct-424145"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Naceur</forename>
                    <surname>Belgacem</surname>
                  </persName>
                  <email type="md5">c91d9850f12edf0693b33f5920be1238</email>
                  <email type="domain">efpg.inpg.fr</email>
                  <idno type="idhal" notation="string">mohamed-naceur-belgacem</idno>
                  <idno type="idhal" notation="numeric">1253655</idno>
                  <idno type="halauthorid" notation="string">924888-1253655</idno>
                  <idno type="ORCID">https://orcid.org/0000-0002-3317-7369</idno>
                  <idno type="ISNI">http://isni.org/isni/0000000384814492</idno>
                  <idno type="VIAF">https://viaf.org/viaf/59170858294407681389</idno>
                  <idno type="RESEARCHERID">http://www.researcherid.com/rid/B-7123-2016</idno>
                  <idno type="GOOGLE SCHOLAR">https://scholar.google.fr/citations?user=1wGsMNsAAAAJ</idno>
                  <idno type="IDREF">https://www.idref.fr/084755202</idno>
                  <idno type="RESEARCHERID">http://www.researcherid.com/rid/http://www.researcherid.com/rid/B-7123-2016</idno>
                  <affiliation ref="#struct-703"/>
                  <affiliation ref="#struct-703"/>
                </author>
                <author role="aut">
                  <persName>
                    <forename type="first">Julien</forename>
                    <surname>Bras</surname>
                  </persName>
                  <email type="md5">ea0a89e6b694a3c781e952cb707ad227</email>
                  <email type="domain">grenoble-inp.frFundingAgencyandGrantNumberInstitut</email>
                  <idno type="idhal" notation="numeric">1070286</idno>
                  <idno type="halauthorid" notation="string">320877-1070286</idno>
                  <affiliation ref="#struct-703"/>
                  <affiliation ref="#struct-703"/>
                </author>
              </analytic>
              <monogr>
                <idno type="halJournalId" status="VALID">14154</idno>
                <idno type="issn">0926-6690</idno>
                <title level="j">Industrial Crops and Products</title>
                <imprint>
                  <publisher>Elsevier</publisher>
                  <biblScope unit="volume">62</biblScope>
                  <biblScope unit="pp">552-559</biblScope>
                  <date type="datePub">2014</date>
                </imprint>
              </monogr>
              <idno type="doi">10.1016/j.indcrop.2014.09.017</idno>
              <idno type="prodinra">278895</idno>
              <idno type="wos">000345468800075</idno>
              <ref target="https://archives-publications.inrae.fr/278895.pdf" type="seeAlso"/>
              <ref type="publisher">http://www.journals.elsevier.com/industrial-crops-and-products/</ref>
            </biblStruct>
          </sourceDesc>
          <profileDesc>
            <langUsage>
              <language ident="en">English</language>
            </langUsage>
            <textClass>
              <keywords scheme="author">
                <term xml:lang="en">Biorefinery</term>
                <term xml:lang="en">Reinforcement</term>
                <term xml:lang="en">Thermal properties</term>
                <term xml:lang="en">Valorisation</term>
                <term xml:lang="en">Cellulose nanocrystals</term>
              </keywords>
              <classCode scheme="halDomain" n="chim.mate">Chemical Sciences/Material chemistry</classCode>
              <classCode scheme="halTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halOldTypology" n="ART">Journal articles</classCode>
              <classCode scheme="halTreeTypology" n="ART">Journal articles</classCode>
            </textClass>
            <abstract xml:lang="en">
              <p>Agave tequilana and barley by-products from the Mexican food industry were characterized to determine their chemical composition and morphology by scanning electron microscopy (SEM). Cellulose was then extracted by carrying out alkali and bleaching treatments and cellulose nanocrystals (CNC) were isolated by an acid hydrolysis. Structural analyses and thermal stability of the isolated CNC were studied by X-ray diffraction (XRD) and thermogravimetric analysis (TGA), respectively. atomic force microscopy (AFM) and diffusion light scattering (DLS) were used to investigate the morphology of the CNC. The results indicate that hemicellulose and lignin were removed from the extracted cellulose. The isolated CNC from bagasse were found to be longer than those from microcrystalline cellulose (MCC), with a length of 322 ± 112 and 329 ± 123 nm for A. tequilana and barley CNC, respectively, compared to 218 ± 56 nm for CNC from MCC. The degradation temperature of A. tequilana and barley CNC was at least 30 °C higher than CNC from MCC. These values are promising for the value of by-products for the isolation of CNC and their use in reinforced-polymer manufacturing.</p>
            </abstract>
          </profileDesc>
        </biblFull>
      </listBibl>
    </body>
    <back>
      <listOrg type="structures">
        <org type="laboratory" xml:id="struct-135725" status="OLD">
          <orgName>Génie industriel alimentaire</orgName>
          <orgName type="acronym">GENIAL</orgName>
          <desc>
            <address>
              <addrLine>1 avenue des Olympiades, F-91744 Massy</addrLine>
              <country key="FR"/>
            </address>
          </desc>
          <listRelation>
            <relation name="UMR1145" active="#struct-92114" type="direct"/>
            <relation active="#struct-148117" type="direct"/>
            <relation active="#struct-300351" type="direct"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-703" status="OLD">
          <idno type="IdRef">181234564</idno>
          <idno type="ISNI">0000 0004 0384 3417</idno>
          <idno type="RNSR">199511962D</idno>
          <idno type="ROR">https://ror.org/02z8yps18</idno>
          <orgName>Laboratoire Génie des procédés papetiers</orgName>
          <orgName type="acronym">LGP2</orgName>
          <date type="start">1985-01-01</date>
          <date type="end">2019-12-31</date>
          <desc>
            <address>
              <addrLine>461 Rue de la Papeterie - 38402 ST MARTIN D'HERES CEDEX</addrLine>
              <country key="FR"/>
            </address>
          </desc>
          <listRelation>
            <relation active="#struct-89889" type="direct"/>
            <relation active="#struct-300275" type="direct"/>
            <relation name="UMR5518 / URA1100" active="#struct-441569" type="direct"/>
          </listRelation>
        </org>
        <org type="laboratory" xml:id="struct-424145" status="INCOMING">
          <orgName>CA Quimica de Alimentos - Centro de Investigaciones Quimicas</orgName>
          <desc>
            <address>
              <country key="MX"/>
            </address>
          </desc>
          <listRelation>
            <relation active="#struct-237606" type="direct"/>
          </listRelation>
        </org>
        <org type="institution" xml:id="struct-92114" status="OLD">
          <idno type="ROR">https://ror.org/01x3gbx83</idno>
          <orgName>Institut National de la Recherche Agronomique</orgName>
          <orgName type="acronym">INRA</orgName>
          <date type="start">1946-05-18</date>
          <date type="end">2019-12-31</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.inra.fr</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-148117" status="VALID">
          <idno type="IdRef">139408088</idno>
          <idno type="ROR">https://ror.org/02kbmgc12</idno>
          <orgName>AgroParisTech</orgName>
          <date type="start">2007-01-01</date>
          <desc>
            <address>
              <addrLine>22 place de l'Agronomie CS 20040 91123 Palaiseau cedex</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.agroparistech.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-300351" status="VALID">
          <idno type="IdRef">027404978</idno>
          <idno type="ISNI">0000000121690459</idno>
          <idno type="ROR">https://ror.org/0175hh227</idno>
          <orgName>Conservatoire National des Arts et Métiers [Cnam]</orgName>
          <orgName type="acronym">Cnam</orgName>
          <desc>
            <address>
              <addrLine>292 Rue Saint-Martin, 75003 Paris</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.cnam.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-89889" status="OLD">
          <idno type="IdRef">026388804</idno>
          <idno type="ROR">https://ror.org/05sbt2524</idno>
          <orgName>Institut polytechnique de Grenoble - Grenoble Institute of Technology</orgName>
          <orgName type="acronym">Grenoble INP</orgName>
          <date type="start">2007-01-01</date>
          <date type="end">2019-12-31</date>
          <desc>
            <address>
              <addrLine>46 avenue Félix Viallet 38031 Grenoble Cedex 1</addrLine>
              <country key="FR"/>
            </address>
            <ref type="url">http://www.grenoble-inp.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-300275" status="OLD">
          <idno type="IdRef">026388804</idno>
          <orgName>Institut National Polytechnique de Grenoble</orgName>
          <orgName type="acronym">INPG</orgName>
          <date type="end">2006-12-31</date>
          <desc>
            <address>
              <addrLine>46 avenue Félix Viallet 38031 Grenoble Cedex 1</addrLine>
              <country key="FR"/>
            </address>
          </desc>
        </org>
        <org type="regroupinstitution" xml:id="struct-441569" status="VALID">
          <idno type="IdRef">02636817X</idno>
          <idno type="ISNI">0000000122597504</idno>
          <idno type="ROR">https://ror.org/02feahw73</idno>
          <orgName>Centre National de la Recherche Scientifique</orgName>
          <orgName type="acronym">CNRS</orgName>
          <date type="start">1939-10-19</date>
          <desc>
            <address>
              <country key="FR"/>
            </address>
            <ref type="url">https://www.cnrs.fr/</ref>
          </desc>
        </org>
        <org type="institution" xml:id="struct-237606" status="VALID">
          <orgName>Universidad Autónoma del Estado de Hidalgo</orgName>
          <orgName type="acronym">UAEH</orgName>
          <desc>
            <address>
              <country key="MX"/>
            </address>
            <ref type="url">https://www.uaeh.edu.mx/</ref>
          </desc>
        </org>
      </listOrg>
      <listOrg type="projects">
        <org type="anrProject" xml:id="projanr-37552" status="VALID">
          <idno type="anr">ANR-11-LABX-0030</idno>
          <orgName>TEC XXI</orgName>
          <desc>Ingénierie de la Complexité : la mécanique et ses interfaces au service des enjeux sociétaux du 21iè</desc>
          <date type="start">2011</date>
        </org>
      </listOrg>
    </back>
  </text>
</TEI>