Biomolecular Solid-State NMR/Basics
Résumé
Solid-state NMR spectroscopy has significantly grown in recent years thanks to combined progress in sample preparation, probe and magnet technology, and radiofrequency irradiation schemes; the field is now open to the structural characterization of systems that are highly pertinent to many areas of modern biology. This chapter presents an outline of the basic steps in the magic angle spinning solid-state NMR experiments available today - cross-polarization, heteronuclear decoupling, and homonuclear recoupling.