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              <p>Fine scale microstructure and hardness properties of bulk Zn-Al-Mg alloys have been investigated after solution-annealing, during ageing at room temperature and after ageing at 95 degrees C. Small-angle X-ray scattering measurements evidence nucleation, growth and coarsening of tiny elongated precipitates (probably of the (Al) phase) in Zn-Al-Mg alloys during ageing, with a characteristic size of 10 nm, and a characteristic time scale of 1 h at 95 degrees C to complete the precipitation reaction. Small additions of magnesium strongly enhance this precipitation. A strong effect on both hardness and two-stage precipitation enthalpy was evidenced. The nodules of both alpha-(Al) and eta-(Zn) phases formed by decomposition of the former alpha' phase showed a bimodal size distribution. An ageing treatment at 15 and 95 degrees C mainly affected the bulk of former alpha' particles i.e. the finest areas of this microstructure.</p>
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