Experimental investigation of microstructure and ageing behaviour of bulk Zn-(1-18) wt% Al-(0-0.06) wt% Mg alloys - Archive ouverte HAL Accéder directement au contenu
Article Dans Une Revue Materials Science and Engineering: A Année : 2010

Experimental investigation of microstructure and ageing behaviour of bulk Zn-(1-18) wt% Al-(0-0.06) wt% Mg alloys

Résumé

Fine scale microstructure and hardness properties of bulk Zn-Al-Mg alloys have been investigated after solution-annealing, during ageing at room temperature and after ageing at 95 degrees C. Small-angle X-ray scattering measurements evidence nucleation, growth and coarsening of tiny elongated precipitates (probably of the (Al) phase) in Zn-Al-Mg alloys during ageing, with a characteristic size of 10 nm, and a characteristic time scale of 1 h at 95 degrees C to complete the precipitation reaction. Small additions of magnesium strongly enhance this precipitation. A strong effect on both hardness and two-stage precipitation enthalpy was evidenced. The nodules of both alpha-(Al) and eta-(Zn) phases formed by decomposition of the former alpha' phase showed a bimodal size distribution. An ageing treatment at 15 and 95 degrees C mainly affected the bulk of former alpha' particles i.e. the finest areas of this microstructure.

Domaines

Matériaux

Dates et versions

hal-00542912 , version 1 (03-12-2010)

Identifiants

Citer

B. Wattiez, Anne-Françoise Gourgues, A. Deschamps, A. Roeme, Z. Zermout. Experimental investigation of microstructure and ageing behaviour of bulk Zn-(1-18) wt% Al-(0-0.06) wt% Mg alloys. Materials Science and Engineering: A, 2010, 527 (29-30), pp.7901-7911. ⟨10.1016/j.msea.2010.08.068⟩. ⟨hal-00542912⟩
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