Microstructural study of β treated grade 702 zirconium. Scanning electron microscopy and transmission electron microscopy, complementarity of two observational scales
Résumé
In this study we focus on the precipitation of betagenic elements (Fe, Cr, Ni) that occurs during the β→α allotropic transition in zirconium. In particular its structural characteristics, morphology and their consequences for the mechanical behaviour of the material are probed. The observations are made by means of a scanning electron microscope and a transmission electron microscope. The results reveal the occurrence of a quasi-continuous single crystalline phase, produced by the precipitation of the betagenic additional elements which constitute the so-called lath boundaries. This phase forms a layer surrounding the laths in the bulk of the material. Its morphology could be assimilated to a net, created by precipitates with a size of several micrometres and linked by narrow bridges with a size of several hundred nanometres. The chemical composition of the precipitates are of the Zrx(Cr,Fe2)1-x type with x≤40%.
Domaines
MatériauxOrigine | Fichiers produits par l'(les) auteur(s) |
---|