Microstructural study of β treated grade 702 zirconium. Scanning electron microscopy and transmission electron microscopy, complementarity of two observational scales - Archive ouverte HAL
Article Dans Une Revue Journal of Materials Science Année : 1997

Microstructural study of β treated grade 702 zirconium. Scanning electron microscopy and transmission electron microscopy, complementarity of two observational scales

Jérôme Crépin
Daniel Caldemaison
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Alain Barbu
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Gérard Jazkierowitcz
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Résumé

In this study we focus on the precipitation of betagenic elements (Fe, Cr, Ni) that occurs during the β→α allotropic transition in zirconium. In particular its structural characteristics, morphology and their consequences for the mechanical behaviour of the material are probed. The observations are made by means of a scanning electron microscope and a transmission electron microscope. The results reveal the occurrence of a quasi-continuous single crystalline phase, produced by the precipitation of the betagenic additional elements which constitute the so-called lath boundaries. This phase forms a layer surrounding the laths in the bulk of the material. Its morphology could be assimilated to a net, created by precipitates with a size of several micrometres and linked by narrow bridges with a size of several hundred nanometres. The chemical composition of the precipitates are of the Zrx(Cr,Fe2)1-x type with x≤40%.

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Matériaux
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hal-00111571 , version 1 (01-11-2022)

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Jérôme Crépin, Thierry Bretheau, Daniel Caldemaison, Alain Barbu, Gérard Jazkierowitcz. Microstructural study of β treated grade 702 zirconium. Scanning electron microscopy and transmission electron microscopy, complementarity of two observational scales. Journal of Materials Science, 1997, 32 (18), pp.4841-4846. ⟨10.1023/A:1018603619366⟩. ⟨hal-00111571⟩
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